What is Sour Gas Corrosion Testing?

The exposure of some metallic components to sour (i.e. H2S containing) aqueous environments can potentially lead to corrosion and/or environmentally assisted cracking. Environmentally assisted cracking comprises several specific cracking mechanisms such as sulfide stress cracking (SSC), stress corrosion cracking (SCC) and hydrogen induced cracking (HIC), among others.

All of these cracking mechanisms require a susceptible material, in either a stress or unstressed state, in an aqueous sour environment. NACE (now known as AMPP) has developed several standard test methods that define and create a sour gas containing corrosive environment and standard loading conditions that can be used to help assess a materials’ relative resistance to these various forms of environmentally assisted cracking.

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Why Choose Acuren

Experience

Experience

With over 40 years of experience in this field, our team has developed procedures to ensure that we consistently and repeatedly meet all of these requirements.

In-House Machining

In-House Machining

All our test specimens are machined in-house to ensure consistent fabrication within all specified tolerances and the fastest possible turnaround time to meet our client’s needs.

Quality

Quality

Our sour gas corrosion testing laboratory is ISO 17025 accredited for NACE corrosion testing and ASTM mechanical testing, demonstrating our commitment to technical competence, quality assurance, and internationally recognized testing standards.

Engineering Expertise

Engineering Expertise

Acuren has the largest network of laboratories across North America with specialized engineers who can examine your components for potential damage, perform failure analysis and materials selection to ensure optimal asset reliability.

Specialist CNC operators

Specialist CNC operators

The latest in CNC machining technologies
The latest in CNC machining technologies
Precision optical measuring systems
Precision optical measuring systems

Types Of Sour Gas Corrosion Tests We Perform

NACE TM0177 – Testing of Metals for Resistance to Sulfide Stress Cracking (SSC) and Stress Corrosion Cracking (SCC) in H2S Environments

This test standard provides guidance to assess a material’s resistance to cracking failure under the combined action of applied stress and corrosion in aqueous environments containing hydrogen sulfide (H2S). Several methods of applying stress and assessing performance are provided within NACE TM0177. All require immersion of the test specimen in a low pH, aqueous sour (i.e. H2S containing) environment for a prolonged period of time. Standard test conditions (including 4 standard test solutions) are defined in NACE TM0177 but, custom test conditions can be created to suit your needs.

Method A Tensile Test
NACE Method A Testing Apparatus
Method A: Tensile Test

A simple, unnotched test specimen is loaded in static uniaxial tension (via proof ring) and placed in the environmental test vessel for up 720 hours. The absence of specimen fracture/cracking is acceptable, while cracking or fracture constitutes a failure. By testing a material at different stress levels, an apparent threshold stress level can be determined below which cracking due to SSC would not be expected.

Method C C-Ring Test
NACE Method C Test Specimen
Method C: C-Ring Test

A “C” shaped partial ring of material (typically from a tubular type product) is loaded circumferentially and placed in the environmental test vessel for up to 720 hours. The absence of specimen fracture/cracking is acceptable, while cracking or fracture constitutes a failure. By testing a material at different stress levels, an apparent threshold stress level can be determined below which cracking due to SSC would not be expected.

Method D DCB Test
NACE Method D: Test Specimens
Method D Double Cantilever Beam (DCB) Test

Unlike the pass/fail Methods A and C, the DCB test (Method D) measures resistance to environmentally assisted crack growth as a critical stress intensity factor, KISSC. A wedge loads the specimen at a starter notch before environmental exposure. Valid tests require crack growth (typically after 14 days). Lower-strength materials may need fatigue pre-cracking to initiate cracking.

TM0316 Apparatus
NACE TM0316 Testing Apparatus

NACE TM0316 uses four-point bend testing to assess metals—including carbon steels, low alloy steels, CRAs, and welded or clad materials—for resistance to stress corrosion cracking (SCC) and sulfide stress cracking (SSC).

Specimens are loaded in a four-point bend jig to apply a controlled tensile stress and exposed to one of four standard NACE TM0177 solutions (A–D) or a custom environment. After exposure, samples are examined for cracking.

NACE TM0284 – Evaluation of Pipeline & Pressure Vessel Steels for Resistance to Hydrogen-Induced Cracking

In wet, sour (H₂S) environments, absorbed hydrogen can cause hydrogen induced cracking (HIC), leading to failures in pipelines and pressure vessels. NACE TM0284 tests unstressed samples from pipes and related components in three standard solutions: A and B (96 hours) and C (96 hours to 90 days, depending on H₂S pressure).

Do you fabricate, design, supply, or operate infrastructure in a sour service environment?

If yes, Acuren can test your materials to the following industry standards NACE TM0177, NACE TM0284, NACE TM0284, NACE TM0316. These tests are important to help ensure safe operation of downhole products, pipelines, and storage vessels, and for identifying suitable materials for use in sour, corrosive environments.

Evan Wan
Operations Manager, Sour Gas Corrosion Testing Prairies Region
T  403.250.7081
C  403.608.7915
E  evan.wan@acuren.com

2157 23 Street NE, Calgary, AB, T2E 8J8, CANADA

Contact our Sour Gas Corrosion Testing experts today!

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